Peer-Reviewed Publication
Inorg Chem2026;65(32):18925-18937.August 17, 2026Journal Article
Refinement of the Magnetic Behavior of Nanostructured Ni-Fe-OH Layered Double Hydroxides.
Mariia Holub1,2, Elena L Fertman3, Alexey V Fedorchenko3, Yurii G Pashkevich4, Antoine Barbier5, Razvan Burcea6,7, Brahim Dkhil6, Frédéric Fossard7, Philippe Ohresser2, Cristina S Neves8, Andrei N Salak8, Erik Čižmár9
1Faculty of Physics and Applied Computer Science, AGH University of Krakow, al. A. Mickiewicza 30, 30-059Krakow, Poland.
2Synchrotron SOLEIL, L'Orme des Merisiers, 91192Gif sur Yvette Cedex, France.
3B. Verkin Institute for Low Temperature Physics and Engineering of NASU , 61103Kharkiv, Ukraine.
4O. Galkin Donetsk Institute for Physics and Engineering of NASU, 03028Kyiv, Ukraine.
5SPEC, CEA-Saclay, CNRS, Université Paris-Saclay, 91191Gif-sur-Yvette Cedex, France.
6CentraleSupelec, Université Paris-Saclay, 91191Gif-sur-Yvette Cedex, France.
7Université Paris Saclay, ONERA, CNRS, Laboratoire d'étude des microstructures, 92322Châtillon, France.
8Department of Materials and Ceramics Engineering, CICECO - Aveiro Institute of Materials, University of Aveiro, 3810-193Aveiro, Portugal.
9Institute of Physics, Faculty of Science, P.J. Šafárik University in Košice, 04154Košice, Slovakia.
Abstract
Magnetic properties of OH--intercalated Ni2+-Fe3+ layered double hydroxides (LDH) with a nickel-to-iron ratio (n) of 2 and 3, prepared using two independent synthesis methods, have been studied using the macroscopic magnetic method (SQUID magnetometry) and local-scale element-specific techniques (synchrotron-radiation-based soft X-ray XAS and XMCD). It was revealed that synthesis of NinFe-OH LDH u…
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